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12. Optical Instruments

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INSTRUMENT REPAIRS & MODIFICATIONS (IN ALPHANUMERIC ORDER)

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 #  Action  Status   Problem         Manufacturer     Model           Function

 1  Refurb  TBD      Lethal          Jinan Mao An     JH-B            Hollow Cathode Lamp Activator

 2  Refurb  Fixed    Dim backlight   Laser Precision  Rk-5710         Power Radiometer 0 - 30W

 3  Refurb  Fixed    Dim backlight   Laser Precision  Rj-7610         1-ch Energy Radiometer 0 - 1J

 4  Refurb  Fixed    Dim backlight   Laser Precision  Rj-7620         2-ch Energy Radiometer 0 - 1J

 5  Repair  Fixed    Not working     Laser Precision  RkP-575/Rk-570C Shutter motor control section

 6  Repair  Fixed    Broken switch   Oriel            68806 PSU       Arc lamp PSU

 7  Refurb  Fixed    Bad design      Oriel            Q Series case   Arc lamp holder

 8  Repair  Fixed    Broken lamp     Newport          6251NS          75W Xenon arc lamp

 9  Repair  Ongoing  Inaccurate      Sequoia Turner   340             Spectrophotometer
10  Repair  Ongoing  Bad IR source   Generic          360             FTIR chemistry analyser [TBD]

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1. Jinan Mao An JH-B Hollow Cathode Lamp Activator (Rejuvinator)

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INITIAL INSPECTION 10/03/14 LIBS3 P.10

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This Chinese instrument rejuvenates hollow cathode tubes by using an established method of running a high voltage across them at a controlled current for a specific period of time.

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Unfortunately it has been built to an atrocious standard that renders it lethal, and it needs a rebuild. It is in a plastic box but it has metal end plates. There is no transformer; it runs directly off the mains and no metalwork is earthed. Look at the soldering on the uninsulated mains neon!

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The holes in the metal back are 6mm diameter - big enough to get a fairly large screwdriver through.

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​The BU208A HV transistor is insulated by a mica sheet from its aluminium plate in the bottom of the plastic box. The wire soldered to its case tag with a big amateur blob is hidden by a loose section of heatshrink that hasn't been shrunk. This wire's insulation outside diameter is 1.2mm, and the other end of it is soldered to the centre pin of the POS/NEG DPCO switch without any insulation covering it.​​​​​

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I measured 700V across the HCL and this is directly connected to the pos/neg switch which just swaps polarities so the HCL gets +-700V or -+700V; the uninsulated 1.2mm wire is carrying 700V. The small 'PE Lamp Socket' on the rear panel has exposed contacts that also carry 700V. Terrifying!

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CHANGE THE CHASSIS UNDERSIDE PHOTO/DESCRIPTION - THE BU208A IS INSULATED BY MICA SHEET​

 Front panel               HCL socket on top  Rear no earth & big holes   Instructions    Limits

  Metalwork not earthed    Insecure components       Mains neon no insulation   HV resistors not secured

 Internal metal is live!      Self taps hold pcb!         BU208A poorly insulated        Bad insulation 

 HCL lamp    Reverse-engineered cct      NB 22k pot is 2W (for redesign)

Laser Precision optical power/energy meters - replaced all dimly lit LCD backlights (2022)

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2. Laser Precision Rk-5710 Power  Radiometer up to 30W

3. Laser Precision Rj-7610 Single Energy Radiometer up to 1J

4. Laser Precision Rj-7620 Dual   Energy Radiometer up to 1J

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2013 eBay $14 Chinese EL backlight white 150mm x 50mm x2 for Rj-7610 & Rk-5710
2013 eBay $11 Chinese EL backlight blue  149mm x 44mm x1 for Rj-7620 power meter

2022 eBay $ 6 Chinese EL backlight white 6" x 2"(152mm x 51mm) + inverter x3 for all three meters 

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The electroluminescent backlights in these units are off by default and have to be turned on rather laboriously using the front panel membrane push-buttons, presumably to extend their life. The Rj-7610 has the same PCB as the Rj-7620 but is missing the extra components for the second channel. I found the backlight inverter and circuitry to enable it had been manually wired into to every PCB as a later addition, with different circuits for the Rk-65710 and Rj-76x0. All inverters run off the 5V supply and have an enable pin that must be logic 0 (0V) or floating to turn on the inverter (I assume it has an internal pull-down resistor). All instruments have an 8031 µC and the inverter is enabled via a PNP transistor with its emitter wired to +5V.

In the Rj-76x0 the 8031 µC I/O port on pin 14 drives the base of the PNP transistor. When when the port is driven to a logic 0 (0V) the PNP turns on and drives +5V into the inverter enable pin, turning it on.

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I moved the wire from the µC port pin to its 0V supply pin 20, forcing the inverter permanently on.

The Rk-5710 design is more involved. Its 8031 µC drives a 74139 dual 4:1 decoder, and one of its outputs controls the inverter. Again, the inverter was added later, so its transistor is a manually wired circuit next to the inverter, but it differs by having a 7474 D-type latch configured as a toggle between the 139 and the PNP transistor, see circuit below. A capacitor clears the latch at power-up, forcing the 7474 Q- output to a 1 (+5V), turning off the PNP and disabling the inverter. The 139 output has to transition 0->1 to cause the latch to change state and turn on the inverter, and a second 0->1 transition turns it off. To force the backlight permanently on, I re-wired the PNP base to 0V.

However the intensity of the backlights was too low and in 2013 I replaced them. Initially I fitted a blue one to the Rj-7610 but it wasn't very bright so I fitted white ones to the other two instruments.

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Below, the outside LCD area is about 145mm x 16mm. Inside, the LCD PCB is retained by four Torx 10 screws. The original backlight was soldered to the front of the PCB and two wires soldered to its back lead off to the inverter. Although the inverter output is floating ac, the black wire connects one lead to 0V which is also connected to the chassis metalwork. 

Backlights can be cut to size from larger panels. The cheapest panels were from eBay China and in 2013 the smallest ones I could find that were long enough, were 148mm x 44mm. This was a good thing, because when I removed the LCD PCB I found the original panels measured 152mm x 21mm. If I had bought 16mm wide panels they would have misaligned. I used the original panel as a template and cut the new panel to the same size. The new panels shown below are the 152mm x 51mm ones I bought in 2022.   

By 2022 I was having difficulty seeing all three LCDs. This time I measured light levels and found there were wide differences in brightness levels of identically sized panels. I also noticed once shining through the LCD, there was huge reduction in light intensity compared to a naked panel on the bench.

I replaced all three backlights as before, this time using white panels but they seemed little brighter.

At first I wondered if it was because like the last lot they were from eBay China and this time they came with an inverter yet were half the price I paid in 2013 despite a $/£ drop. I had hoped to buy them cheaper without inverters but now I was glad they were included, because the only easy fix I could think of was to run them at a higher voltage even if it shortens their life (they're not expensive after all) but I didn't want to risk doing this to the original inverters, and leaving those in meant I had a fall-back in case the idea didn't work.

That said, the onboard inverters run off +5V but the Chinese inverters run off +12V and there is no +12V supply.

 

However all meters have a LM340T/7815 TO-220 +15V 1A IC regulator for the analogue circuitry.

I measured the maximum current taken by the new inverters at 12V( 50mA) and 15V (80mA) along with backlight intensity for both a full size 152x52mm panel as well one cut to 152x21mm for the LCD, and checked the +15V supply was unchanged (+15.23V). I concluded the extra 80mA should not be a problem.

I also measured the inverter output voltage from the original inverter and a new Chinese inverter and found they were similar. I only measured one each but when I measured light levels I realised there must be quite a wide tolerance between different inverters.

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Original inverter at  5V no panel ~162Vac, with panel ~ 109Vac

Chinese  inverter at 12V no panel ~148Vac, with panel ~ 108Vac

Chinese  inverter at 15V no panel ~190Vac, with panel ~ ADD Vac

The Chinese inverters aren't marked but I confirmed a working voltage of ~108Vac at 12V, much the same as the 5 Volt ERG LPS-05-2-1 inverter fitted to the Rk-5710. Increasing the inverter input to 15V produced ~160Vac, doubling the current and increasing light intensity of one panel by 32% and the other by 49%. I only measured one inverter; I expect they also have a loose output voltage tolerance.

I added the new inverters and wired the backlights to them instead. Running them at 15V instead of 12V gave a 30% boost in brightness, and I could now easily see the front panel. I stuck the new adhesive-backed inverters onto the metal side panel on each meter to dissipate any heat, and wired them to the +15V regulator MLC de-coupler.

          Rk-5710                            Rj-7610                               Rj-7620

  Original     New inverter          Original     New inverter              Original     New inverter

Above, the meters inside before and after the new inverters were added and wired to 15V.

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Below left, 2022 meter intensities before refurb: Rk-5710 ( 7 Lux), Rj-7610 (12 Lux), Rj-7620 ( 4 Lux) 

Centre & right,  meter intensities  after refurb: Rk-5710 (38 Lux), Rj-7610 (14 Lux), Rj-7620 (25 Lux) 

 

The Rj-7610 is greyed out because at this point it had not yet been refurbished: 

Later in 2022 I refurbished the Rj-7610 too (the sticker is reminding me to disable its onboard inv):

TEST RESULTS

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I had a spare blue full panel from 2013 for comparison and measured similar intensity at lower current. However I don't think this is significant as I found great inconsistency across all panels & inverters.

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        2022 152X52MM ON BENCH       2013 149X44MM ON BENCH       2013 PANEL FROM LCD ON BENCH

        WHITE #1       WHITE #1      BLUE           BLUE          WHITE          WHITE

PSU     Full panel     Full panel    Full panel     Full panel    21mm wide      21mm wide

Volts   PSU current    Intensity     PSU current    Intensity     PSU current    Intensity

 3V     0.5mA           22 Lux        -              -             -               -

 5V      15mA           81 Lux        -              -             -               -

12V      80mA          433 Lux       60mA           633 Lux       30mA           578 Lux            

15V     110mA          567 Lux       80mA           839 Lux       60mA           864 Lux

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        2022 152X52MM ON BENCH       2022 152X21MM IN Rk-5710     2022 152X21MM ON BENCH

PSU     WHITE #2       WHITE #2      WHITE #1       WHITE #1      WHITE #2       WHITE #2

PSU     Full panel     Full panel    21mm wide      21mm wide     21mm wide      21mm wide

Volts   PSU current    Intensity     PSU current    Intensity     PSU current    Intensity

 3V       -              -            -              -             -               -

 5V       -              -            -              -             -               -

12V      80mA          381 Lux       50mA           34 Lux        50mA           592 Lux            

15V     120mA          479 Lux       80mA           38 Lux        80mA           791 Lux

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FINAL RESULTS

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2022 backlight intensity before refurb: Rk-5710 =  7 Lux, Rj-7610 = 12 Lux, Rj-7620 =  4 Lux.

 

2022 backlight intensity  after refurb: Rk-5710 = 38 Lux, Rj-7610 = 36 Lux, Rj-7620 = 25 Lux.

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Right - Lastly I removed my earlier mods to force the onboard inverters on, partly to save power but also because they might not like running without a load.

Left - The lids warp outward unless nylon washers are placed on the mounting screws between the lid and frame, and I finally got round to gluing all 24 in place.

5. Laser Precision combined RkP-575 shutter + Rk-570C optical power probe

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This is a pyro electric probe that measures CW power up to 10W. There was no output signal on arrival.

 

There are two pcbs inside:

The top pcb is a pre-amplifier for the pyro electric sensor on its left (centre photo).

The bottom pcb (right photo) controls the motor to its right that rotates a shutter in front of the detector, effectively synthesising a pulsed waveform into the detector that would otherwise be used to measure energy rather than power.

 

The motor control pcb has a 15µF 20V tantalum capacitor C201 (arrowed in photo, right) across the +15V supply line that comes from the pre-amp board through a short external lead via the RJ-45 connector on each pcb. This capacitor was a dead short.

Capacitor C201 replaced with a new 15µF 20V tantalum, unit tested and operational.

6. Oriel Instruments 68806 arc lamp PSU & xenon lamp repair (2018)

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[D18] Manual for Oriel Model 6000 Q series Lamp housing

http://www.newport.com/p/6251NS

Newport 6251NS Xe 14V 5.4A 75W arc lamp

Oriel   6251   Xe 14V 5.4A 75W arc lamp

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I bought an Oriel 68806 50-200W Basic arc lamp PSU, Q Series lamp housing and two new 75W Xe arc lamps to provide a (low power) deep UV source for general measurement - see above URL and spectrum below. Newport ignored me when I asked what the NS means in their part number; 'Newport Special'?

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This is my low cost alternative to a deuterium lamp which from what I have read has a limited shelf life in the order of about 2 to 5 years; 'D2 lamps *do* have a finite shelf life as D2 can diffuse past glass-to-metal seals.', found here: https://www.chromforum.org/search.php?keywords=deuterium+shelf+life

There are many very old D2 lamps particularly of USSR origin for sale on eBay that will not work, and any modern lamp over 5 years old is also unlikely to work.

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Amongst other things, when combined with a monochromator I shall use this Xenon arc lamp to verify luminescence of UV to VIS image converters that will later be used to verify UV laser emissions without endangering the Stellarnet (any exposure to UV is harmful, so I limit it).

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The PSU VOLTS/AMPS switch toggle was broken off and I replaced it. It came with a Cramer hour timer but when I changed the PSU voltage selector to 230Vac for UK mains, I discovered despite being hard wired into the supply, the timer was only rated for 115Vac so I removed it. I was impressed that after being driven at twice its rated voltage, its 60Hz synchronous motor still worked at 115Vac, albeit 50Hz.

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The PCB PSU bottom brown capacitor next to the yellow transformer looks like it's bulging, but I found this was only the outer plastic cover and not the internal aluminium case, so I ignored it:

Above: 6251NS arc lamp spectrum

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Below: Cramer hour timer

Above: inside photo

The Cramer is wired to the main switch bottom left and exits right

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Left/right: the broken switch is located below the meter top left

The lamps came with numerous safety notices warning the high pressure could result in an explosion if roughly handled. The Oriel 6000 lamp housing manual actually specifies it is for use with the 6251 lamp but when I assembled the lamp I was surprised the design involves a heavy brass slug at the top with no means of support. Furthermore whilst the external cables to the PSU are EHT rated extra flexible silicone, the internal ones are high voltage rigid cables that are difficult to align without putting stress on the lamp. I put it together but couldn't help thinking the design was idiotic, and made a special effort to arrange the lamp wiring exactly as recommended in the Oriel manual for the housing:

Below - I fired it up and took a few measurements. After about 30 minutes I confirmed the presence of DUV down to the 185nm limit of the Stellarnet, then turned the lamp off and left it to cool down.

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PSU & lamp working fine:               UV down to 185nm:              Full spectrum:

Left: A label on another arc lamp warns not to restart the lamp within 30 minutes. I assumed it would also not be a good idea to move it for that time, so I left it a good hour before I moved it back to storage.

 

Just as I lifted it up to put it on its shelf, there was an ominous rattle from inside. Dismantling it, I found the arc lamp had severed at the bottom, straight through the glass where the internal cathode lead was sealed within it, with the pressurised envelope above it still intact.

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As I had feared, the weight of the solid brass anode slug at the top of the lamp had snapped the new $50 eBay lamp in two (they're over $300 new). At least it didn't explode.

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I wasn't going to risk the second lamp until I had a better construction, which meant I would have to modify it first.

7. Lampholder re-design

The housing is convection cooled so I had to avoid obstructing the heat rising off the lamp. I built a scaffold using a strip of fibreglass PCB sheet clamped at the bottom, supporting two carbon fibre tubes each side, with a solid but heat-expandable flexible support for the brass anode at the top.

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8. Xenon lamp repair​

I also wondered if I could get the broken lamp to work if it was still pressurised. I really needed some kind of electrically conductive TIM (Thermal Interface Material) between the broken halves of its bottom contact still in its glass body. Mercury was a possibility but it's toxic. It occurred to me gallium might be a suitable choice as unlike Hg it readily wets metal and glass, its resistance is 270nΩ/m at 20°C and it melts at 29.76°C (85.57°F, 302.9K) but only boils at 2400°C (2676K). I bought a 10g syringe of it from eBay China for $4 to try out my idea.

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https://en.wikipedia.org/wiki/Gallium

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March 2018: Success! See photos below, left to right in chronological sequence: hover over (or click on) each photo for its description.

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Gallium permeates metals rendering them brittle: I have yet to see how long this novel repair will last.

Oriel arc lamp support scaffold

Oriel 6000 lamp housing
[D18] Oriel 6000 Lamp housing Q manual

http://www.newport.com/p/6251NS

Newport 6251NS Xe 14V 5.4A 75W arc lamp

Oriel   6251   Xe 14V 5.4A 75W arc lamp

9. Sequoia Turner 340 spectrophotometer

 

A very nice, clean spectrophotometer complete with the full set of filters that is usually missing. Having found a service manual with schematics available online at a professional stockist in the USA, I bought the instrument but when I tried to buy the manual I was told it had been lost in a fire. I have a basic manual with a calibration procedure but no schematics.

 

Calibration cannot be accomplished because the expected results cannot be achieved. This may be due to potentiometer or power supply issues, a faulty detector (embedded deep within the instrument), or the lamp may simply need replacing:

 

Google AI, 2026:

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When the front-panel 100% T/ 0A coarse/fine potentiometers or internal trim pots 'bottom out' (reach their physical end points) on a vintage single-beam instrument like the Sequoia-Turner Model 340, it indicates that the analog control circuit can no longer supply enough voltage gain or offset compensation to bridge the signal gap. Because the system cannot reach a baseline balance point, you must diagnose the hardware bottleneck driving the signal out of bounds.

 

1. Drastically Low Light Output (Most Common)
If the potentiometer is maxed out trying to reach 100.0% T or .000 A, the detector is likely starved for photons and the electronics is trying to boost a near-nonexistent signal.

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Ageing tungsten/halogen lamp: an old bulb will suffer from envelope blackening or filament sagging. It may still glow bright to your eyes, but its actual lumen output - especially near the 340nm to 400nm UV threshold - drops significantly. Fix: Replace the lamp and precisely re-align it to focus the beam directly onto the entrance slit.

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2. High Dark Current / Electronic Drift
If the potentiometer is bottomed out while trying to adjust the Zero Set (0.0% T) with the sample chamber closed:

 

Stray Ambient Light Leak: If the sample compartment lid or housing gasket is warped, ambient room light is flooding the photodiode. The circuit cannot counter this excess signal. Fix: Test the zero-point calibration in a completely darkened room.

 

Failed Power Supply Rail: The internal operational amplifiers rely on stable dc voltage rails. If the smoothing capacitors in the power supply have dried out and drifted, the internal voltage reference shifts. This pushes the adjustment window completely outside trimpot physical reach.

 

3. Component Failure inside the front panel potentiometers
potentiometers from the 1980s are prone to structural breakdown:

Cracked Carbon Track: The internal resistive track can develop dead spots or crack at the end terminals. When the internal slider hits this break, the resistance jumps to infinity (open circuit).

 

Fix: Turn off the power and spray an electronic contact cleaner directly inside the potentiometer housing, then rotate the knob fully back and forth 30 times. If a multimeter test across the outer pins reveals a completely unstable or non-existent resistance profile, the potentiometer must be desoldered and replaced.

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To isolate the exact hardware failure, let me know:
Is the trimpot maxed out while trying to set Zero (0.0% T) or while trying to set 100% T / 0.000 ABS?
At what wavelength (e.g. 340nm or 550nm) are you running into this barrier?
Knowing this will help narrow down whether the issue is a dying lamp or a failing circuit board component.

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LAMP REPLACEMENT

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The original Sequoia-Turner 330-058 / N-7506-L0 bulb is a highly specific 6V, 10W prefixed tungsten lamp with a specialized flanged pre-focus collar (P15d base).

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Because the physical mounting bracket on the Model 340 relies on this collar to sit precisely in the focal center of the monochromator entrance slit, trying to fit a standard pin-base generic halogen bulb (like a G4 or GY6.35 bi-pin) will not work without extensive machining.

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If you are sourcing a generic, budget-friendly cross-reference bulb, you need to match these parameters to make sure the filament lines up perfectly:

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Generic Cross-Reference & Industry Part Numbers

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Instead of looking up 'Sequoia-Turner', search universal industrial lighting or medical bulb catalogs using the following standard designations:

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Industry Standard Code: #7506 or #1201 (Verify it is the 6V 10W pre-focused miniature version, as some automotive bulbs share similar base numbers but run at 12V/21W, which will fry the internal power circuit).

 

I seem to remember the bulb in it is a standard automotive part. Maybe the original bulb failed and the previous owner replaced it with a basic bulb like above? I need to recheck this first.

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Base Type: P15d-3 (or standard P15d single-contact flanged base).

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new session:​

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Are you saying an automotive 6V 10W bulb should still work and I don't have to pay $65+ shipping to get the twin N-7506-L0 pack from Nova Biotech usa?

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https://www.novabiotech.com/index.php?main_page=product_info&cPath=920_936&products_id=2156

 

Yes, exactly. A generic 6V 10W automotive/motorcycle bulb with a P15d-3 base will work perfectly fine, and you can absolutely save yourself the $65+ international shipping fee. [1]

Because your Sequoia-Turner Model 340 has an intact, fully adjustable lamp mount, you have all the hardware needed to compensate for the slight manufacturing tolerances of a generic vehicle bulb. [1]

 

Critical Buying Check

B

efore you hit buy on any UK listing, look closely at the product image or description:

 

Look at the bottom contact: It must have only one solder dot on the very bottom tip. If it has two dots, it is a dual-filament bulb (like a 10W/10W high/low beam), which will draw too much current and stress your power board.

 

Verify the wattage: Ensure it says strictly 10W

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How to Peak the Light Path using a Generic Bulb

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Once you physically twist the new 6V 10W bulb into the rear-locking socket, you will use the machine's own digital display to mechanically "focus" it: [1]

 

Power up: Turn the mode switch to TRANS (Transmittance) and allow the machine to warm up. [1, 2]

 

Set a mid-range wavelength: Dial the wavelength knob to a highly visible value (e.g., 540nm or 550nm).

 

Loosen the mount: Look for the adjustment screws on the internal lamp bracket assembly. Loosen them just enough so that you can carefully slide, pivot, or pitch the lamp housing manually. [1]

 

Watch the Display: While keeping your hands clear of the direct light path, slowly manipulate the adjustable bracket. Watch the digital readout on the front of the machine. Your goal is to find the physical position that makes the Transmittance percentage jump as high as possible.

 

Lock it down: Once you find the "peak" position where the numbers stop rising, tighten the mount screws back down. [1]

 

Because a 6V 10W bulb will finally be emitting a bright, full-spectrum white light at the exact correct intensity, peaking the mount like this ensures the optical path catches the beam perfectly. Your calibration pots will immediately drop back into their normal operating range instead of forcing against the end stops.

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Critical Specifications Checklist

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If you find a generic bulb with the right base, confirm it meets these criteria before firing up the instrument: Voltage: 6.0V ac/dc (The 340 power supply transformer yields a tight 6V rail; using a 12V generic bulb will result in a dim, orange glow that won't have enough photon energy to clear the 340nm calibration limit).

 

Wattage: 10W Max (Do not exceed 10W. Moving to a 20W bulb will cause the internal power regulation board to overheat and burn out the power transistors).

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Filament Shape: C-2R or standard horizontal coil.

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Alignment Troubleshooting After Retrofit

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Even with an identical generic base, minor production shifts in a budget lamp's filament position can throw your light beam slightly offline. Once installed, follow this sequence:


1. Turn the instrument on and set the wavelength to 550nm (the middle of the green spectrum, making the light cleanly visible to the human eye).
2. Take a piece of white card stock and place it right over the entrance slit inside the housing.
3. If the projected light spot appears crescent-shaped, off-centre, or fuzzy, gently adjust the housing spring tension screws until the beam narrows into a sharp, bright, concentrated focal point directly over the slit opening.


Once centered, your 100% T potentiometers should cleanly recover their functional mid-range adjustments.
 

CHECK ALSO IF I HELD THE ZERO BUTTON DOWN WHILE I ROTATED the % KNOB OR IF GAI (BELOW) GOT THIS WRONG:

 

The official Sequoia-Turner Model 340 operator text divides calibration into two specific procedural steps: the electronic Zero Set Calibration and the optical 100%T baseline calibration.
Because your adjustment potentiometers are stuck at their endpoints, reviewing the exact mechanical relationship of the controls explains why the knobs are bottoming out.

 

1. The Zero Set (0.0% T) Electronic Calibration
 

The zero adjustment on the Model 340 relies on a coupled mechanical action. You cannot just turn the knob; a spring-loaded switch must be triggered to loop the circuit:
 

The Factory Procedure:
a) Toggle the MODE SWITCH to TRANS.
b) Leave the sample compartment completely empty and close the lid.
c) Press and hold down the physical ZERO SET button (this is usually a button built directly into or directly adjacent to the zero knob).
d) While keeping that button firmly pressed, turn the ZERO knob until the digital display settles exactly on 0.0 % T.

 

Why your pot is bottomed out:

If you try turning the Zero knob without fully pressing and holding that internal button, you are fighting an open electronic circuit. The board will not register the resistance change, causing you to spin the potentiometer until it hits its physical endpoint.

 

2. The 100%T / 0A Gain Calibration
Once the zero point is locked, the machine uses a dual-concentric potentiometer assembly to calibrate the top end of the scale:

 

The Factory Procedure:
a) Insert your blank cuvette (filled with distilled water or your reference solvent) into the sample holder.

b) Keep the machine in TRANS mode.
c) Locate the 100%T/0A adjustment assembly. This consists of two knobs stacked on top of each other on a single shaft: the larger rear ring next to the panel is for Coarse setting, and the smaller front knob is for Fine setting.
d) Turn the larger coarse ring first to get the display close to 100.0.
e) Use the smaller front knob to dial it exactly to 100.0.

 

Why your pot is bottomed out: If the smaller fine-tuning knob was spun all the way to its end stop by a previous user, the coarse ring cannot compensate.

 

How to Reset and Break the Endpoint Loop
To unlock your potentiometers and determine which circuit is failing, follow this specific reset sequence:
a) Turn the instrument off.
b) Spin the Fine 100%T knob and the Coarse 100%T ring backward until they are roughly in the exact middle of their physical rotation range.
c) Turn the ZERO knob to its middle position.
d) Turn the power back on and let it warm up.
e) Attempt Step 1 (Zero Set), making sure to firmly hold down the ZERO SET button while you turn the knob.

 

When you try this reset sequence, let me know:
Does the display change at all when you turn the ZERO knob while holding down the ZERO SET button?
If the zero point calibrates correctly, does the display get stuck below 100% or above 100% when you turn the Coarse 100%T ring?

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(a) Inaccurate and cannot calibrate it (schematics unavailable).

Sequoia Turner 340 Spectrphotometer

10. Broken IR source for FTIR chemistry analyser (2026)

 

In 2025 I noticed FTIR chemistry analysers had dropped in price on eBay and I bought one, only for its IR source to break in transit due to the US seller not bothering to add any packaging whatsoever. I assume he thought once I'd paid the still considerable sum and he'd sent it to me, it was no longer his responsiblity. He also refused to take it back, which meant eBay stepped in and gave me a full refund.

Return shipping was $250 and the seller only insured it for $200, so I guess that's what he paid for it.​

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(a) Custom IR energy source broke in transit.

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 Below left: damaged IR element and initial quick fix          Below right: eBay 23 turn 7R1 IR element

712jF01 P1140920 closeup of IR element broken wire
712jF02 P1140726 closeup of IR element wire repair
712jF03 P1140900 FTIR repair wire strand is 0.15mm thick
712jF04 P290006 ebay IR source (7R1 measured)
712jF05 P290003 eBay IR source has 23 turns

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µ Ω ± ° ⌠ ⌡ ∫ │ ─ √ φ θ Θ ∂ δ ζ ξ ς λ ψ ω  τ µ  Ω ∆ Δ ∑ ∏ π Ξ ○ ≠ ³ ² ± 

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